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1、，沁聲次掌碩士學(xué)位論文論文題目固體硫酸羚胺和鹽酸羚胺的制備作者姓名呂俊英指導(dǎo)教師何潮洪教授學(xué)科專(zhuān)業(yè)化學(xué)工程所在學(xué)院材料與化學(xué)工程學(xué)院提交日期加介次掌碩士學(xué)位論文論文題目固體硫酸羚胺和鹽酸羚胺的制備作者姓名呂俊英指導(dǎo)教師何潮洪教授學(xué)科專(zhuān)業(yè)化學(xué)工程所在學(xué)院材料與化學(xué)工程學(xué)院提交日期二四年十二月浙江大學(xué)碩卜學(xué)位論文固體硫敵輕胺和鹽敵經(jīng)胺的開(kāi)發(fā)日錄，摘要………………，，，前言………………第一章文獻(xiàn)綜述……，……課題背景……，……，……研究此課題的意義··············································一‘‘，，‘、、·················
2、··········二二“………………羚胺及其鹽的用途羚胺及其鹽的結(jié)構(gòu)和性質(zhì)……”文獻(xiàn)綜述……固體羚胺鹽的分離提純···········……一··········……」酮肘的合成本課題研究的目的與方案·······································……本課題研究的目的···························，···············……，···············實(shí)驗(yàn)方案的確定…………第二章溶析法制硫酸羚胺……，·····························，···············……，實(shí)驗(yàn)原理…………實(shí)驗(yàn)過(guò)
3、程……，……，原料…………相關(guān)物質(zhì)的物性參數(shù)······························……分析方法和指標(biāo)計(jì)算……試驗(yàn)裝置……，、、實(shí)驗(yàn)操作……………………結(jié)果與討論……，·································甲醇與原液容積比的確定…………氨水加入星對(duì)產(chǎn)品純得率的影響……反應(yīng)溫度對(duì)產(chǎn)品純得率的影響……，……反應(yīng)時(shí)間對(duì)產(chǎn)品純得率的影響……母液值對(duì)產(chǎn)品純得率的影響……穩(wěn)定性，……試驗(yàn)……宕浙江大學(xué)碩學(xué)位論文固體硫酸輕胺和鹽酸徑胺的開(kāi)發(fā)本章小結(jié)……第二章··········································……酮肪
4、水解制鹽酸羚胺反應(yīng)機(jī)理……實(shí)驗(yàn)過(guò)程……原料……相關(guān)物質(zhì)的物性參數(shù)················································……················································分析方法和指標(biāo)計(jì)算……·····…試驗(yàn)裝置…，實(shí)驗(yàn)操作…………結(jié)果與討論……，·············……鹽酸羚胺合成小試結(jié)果與討論……‘酮肘合成小試結(jié)果與討論……本章小結(jié)……，……，……，……，…‘········································第四章酮肘設(shè)計(jì)及業(yè)化……設(shè)計(jì)依據(jù)…，……，……
5、……，……，··································……丁酮肪生產(chǎn)藝流程產(chǎn)品及原材料質(zhì)量指標(biāo)·············································……，·······································產(chǎn)品及原材料質(zhì)最指標(biāo)…………裝置規(guī)模和原材料的供應(yīng)···············································……物料平衡與二廢處理要點(diǎn)……，……，·、·，·············、·····、··················……土要設(shè)備的計(jì)算和選烈原則
6、……、……，……藝控制指標(biāo)……，……，……測(cè)量?jī)x表與白動(dòng)控制設(shè)計(jì)要點(diǎn)……，……，············……一‘酮肪生產(chǎn)技術(shù)規(guī)程……，……，……，……，本章小結(jié)………第五章結(jié)論……參考文獻(xiàn)……，……浙江人學(xué)碩卜學(xué)位論文固體硫酸經(jīng)胺和鹽酸經(jīng)胺的開(kāi)發(fā)摘要，，本文以低濃度硫酸輕胺為原料測(cè)定了硫酸錢(qián)和硫酸輕胺的沉淀曲線進(jìn)行了溶析法制備固體硫酸輕胺、丁酮肪化水解法制備固體鹽酸輕胺的小試研究，沉，，，淀曲線表明與的沉淀分率隨甲醇與水相的比例的加大而增加時(shí)，隨的增加而迅速增加時(shí)，隨的增，、。，，，加變化不明顯時(shí)的沉淀分率的沉淀分率。在溶析法制備固體硫酸輕胺研究中，考察了甲醇及氨水加入量、反應(yīng)溫度
7、、反應(yīng)時(shí)間、值對(duì)硫酸輕胺收率和純度的影響，得到優(yōu)化的工藝條件為以硫酸經(jīng)胺稀溶液為基準(zhǔn)甲醇加入量、氨水加入量，反應(yīng)溫度約‘℃，反應(yīng)時(shí)間約，值約，在該條件下，硫酸輕胺的收率達(dá)、純度達(dá)。在酮肪水解法制備固體鹽酸輕，、，胺研究中比較了丙酮肪丁酮肪和環(huán)己酮肪對(duì)產(chǎn)品收率的影響優(yōu)選丁酮肪進(jìn)行了較深入的研究，考察了丁酮肪和濃鹽酸的摩爾比、反應(yīng)溫度和時(shí)間對(duì)鹽酸輕，在摩爾一、℃、時(shí)間一，胺產(chǎn)品收率的影響比溫度約小時(shí)的條件下收率可達(dá)左右。在丁酮肪合成研究中，考察了丁酮與硫酸經(jīng)胺的總摩爾、，
