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1、AbstractTheefficientanti—winklereagentBTCAistoocostlytobewidelyused.Sointhisresearch,allalginatederivativesPGAissynthesized.ThenthePGAmixedwithBTCA,CAisusedintheanti—creasefinishingofcottonfabrics.ThesynthesistechnicalityofPGAisconfirmedbyasingle-factorexperi
2、mentatfirst.Thenthereactionproductisconfirmedbyinfraredspectrum.Withthechangeofhydrochloricacid,reactiontemperature,reactiontimeandrotatespeed.ThebestsynthesistechnicalityofPGAisconfirmedherebyacross—cutexperiment.Theresultsshowthatintheeaseoffullyexcessiveep
3、oxypropane,thebestratiobetweensodiumalginateandhydrochloricacidis1:3,thedosageofhydrochloricacidisaround15ml,reactiontemperatureis50"C,rotatespeedis40r/min,andreactiontimeis8h,theyieldofPGAis71.2%.TheeffectoftheamountofPGA,BTCA,differentcuringtemperatureandcu
4、ringtimeoncottonfabricisconfirmedherebyasingle—factorexperimentatfirst.TheresultsshowthatitisfeasibletouseBTCAasacross—linkingagentwithPGAinthecottonanti—wrinklefinishingtechnologies,thistechnologycanraisethecottonfabric’Swrinklerecoveryanglearound800,butthef
5、abrictouchandstrengthwillbedecrease.WiththechangeoftheamountofPGA,BTCA,differentcuringtemperatureandcuringtime,afour-factororthogonalfour-levelprocessingofthecotton.Bymeasuringthecreaserecoveryangle,whiteness,tearstrengthandotherpropertiestodeterminethebestpr
6、ocess.Theresultsshowedbytheorthogonalexperimentalresultsandrangeanalysisoftheoptimumpreparationconditionsis:PGAis15egL,BTCAis40egL,curing150sunder190"C.CreaserecoveryangleofthetreatedcottonfabricCflIlbe265。.Themechanicalpropertiesofthefinishedfabricsdecreases
7、ignificantlywhenbeenwashed.ThenthePGAmixedwithcitricacidisusedintheanti-creasefinishingofcottonfabrics.ChangetheamountofPGA,citricacid,differentcuringtemperaturesandcuringtime.Bymeasuringthecreaserecoveryangle,whiteness,tearstrengthandotherpropeaiestodetermin
8、ethebestprocess.ResultsshowthattheyellowingtendencyofcottonfabricstreatedbyPGAandCAmixtureisimproved.Theresultshowedbytheorthogonalexperimentalresultsandrangeanalysisoftheoptimumpreparati