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1、摘要摘要對(duì)鑄態(tài)AZ80和Mg.Gd-Y鎂合金進(jìn)行了熱擠壓變形,并對(duì)擠壓后的AZ80鎂合金進(jìn)行了410℃×4h固溶+170℃×45h時(shí)效處理,對(duì)Mg-Gd.Y合金采取了225℃×40h時(shí)效處理。采用金相顯微鏡(OM)、掃描電子顯微鏡(SEM)和透射電子顯微鏡(TEM)對(duì)鎂合金的微觀組織進(jìn)行了觀察;采用x射線衍射儀(XRD)對(duì)合金中的相進(jìn)行了鑒定;利用硬度實(shí)驗(yàn)測(cè)試了材料的力學(xué)性能;采用機(jī)械動(dòng)態(tài)分析儀(DMA)測(cè)試了這兩種鎂合金在不同處理狀態(tài)下的阻尼性能,并探討了微觀組織變化對(duì)阻尼性能的影響規(guī)律與機(jī)制。
2、結(jié)果表明,AZ80和Mg.Gd.Y合金在熱擠壓過(guò)程中發(fā)生了再結(jié)晶,擠壓后晶粒尺寸細(xì)小、均勻,晶界上存在少量未完全溶解的析出相,晶粒內(nèi)部位錯(cuò)密度較低。AZ80合金固溶后晶粒長(zhǎng)大,仍有部分未完全溶解的Mgl7A112存在。時(shí)效處理后,溶質(zhì)原子以第二相M917A112的形式沿晶界析出,隨著時(shí)效時(shí)間的延長(zhǎng),析出相富集于晶界處并逐漸聚集長(zhǎng)大,強(qiáng)化效果降低。Mg.Gd-Y合金由于溶質(zhì)原子含量高,時(shí)效過(guò)程中析出M924Y5和MgsGd兩相,時(shí)效硬化效果明顯,3.5h即達(dá)到硬度最大值,形成較尖銳的時(shí)效硬化峰。AZ
3、80和Mg-Gd.Y鎂合金的阻尼性能對(duì)應(yīng)變振幅的依賴性均表現(xiàn)出應(yīng)變振幅獨(dú)立和應(yīng)變振幅依賴兩個(gè)部分,并且可以采用G—L位錯(cuò)釘扎模型給予很好的解析。對(duì)阻尼.溫度.頻率曲線的研究表明,AZ80和Mg.Gd.Y鎂合金的阻尼性能隨測(cè)試溫度和頻率的增加而提高,并且分別于50~100℃和150~200℃范圍內(nèi)出現(xiàn)兩個(gè)阻尼峰。50—100℃時(shí)出現(xiàn)的阻尼峰來(lái)源于合金內(nèi)部位錯(cuò)在基面的運(yùn)動(dòng),而150—200℃范圍內(nèi)出現(xiàn)的阻尼峰則歸因于相界面的微滑移。關(guān)鍵詞:阻尼性能;鎂合金;G.L位錯(cuò)模型大連交通大學(xué)工學(xué)碩士學(xué)位論文A
4、bstractAs-castAZ80andMg·Gd-Ymagnesiumalloyswerehotextruded,andthenasolidsolutionof410"C×4hwithaagingtreatmentof170。C×45hwerecarriedouttoas—extrudedAZ80,andaagingtreatmentof2.25℃×40hwerecarriedouttoas—extrudedMg—Gd-Y.Themicrostructuresofthemagnesiumall
5、oysindifferentstatewereobservedbymeansofOpticalMicrograph,ScannerElectronMicroscope,andTransmissionElectronMicroscope.Themechanicalpropertiesweretestedbyhardnesstest,andthedampingcapacitiesweremeasuredbydynamicmechanicalanalyzer.Theresultsshowedthatth
6、easextrudedalloyswerecomposedoffinegrainsandafewsecondphases,revealingtheoccurrenceofrecrystallizationduringhotextrusion.Dislocationsinalowdensitywereobserved.ThegrainsofAZ80alloygrewduringsolidsolutiontreatment,andtherestillexistedfewsecondphase,Mgl7
7、All2,afterthetreatment.Thesoluteatomsprecipitatedalongthegrainboundaryintheformofthesecondphase,MglTAll2.Theprecipitationgrewlargerwithaover-elongatedagingtime,leadingtoareducingofhardness.Becauseofthehighsolubilityofsoluteatomsandthetwoprecipitatedph
8、ases,i.e.M盟4YsandMgsGd,theMg—Gd-Yalloyexhibitedaobviousaging-hardeningphenomena,andasharppeakappearedwithin3.5hduringtheagingprocess.Theinvestigationofthestrainamplitudedependentdampingcapacityindicatedthatthecurvesshowedstrainamplitudedepende