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1、THEFLORIDASTATEUNIVERSITYCOLLEGEOFARTSANDSCIENCESATWISTONPACKINGANALYTICALCOLUMNSFORREVERSEDPHASELIQUIDCHROMATOGRAPHYByJ.PAULMCCALLADissertationsubmittedtotheDepartmentofChemistryandBiochemistryinpartialfulfillmentoftherequirementsforthedegreeofDoctorofPhilosophyDegreeAwarded:FallS
2、emester,2004ThemembersoftheCommitteeapprovetheDissertationofJ.PaulMcCalldefendedonOctober7,2004._________________________JohnG.DorseyProfessorDirectingDissertation_________________________JodeeL.DorseyOutsideCommitteeMember_________________________WilliamT.CooperCommitteeMember____
3、_____________________AlbertE.StiegmanCommitteeMemberTheOfficeofGraduateStudieshasverifiedandapprovedtheabovenamedcommitteemembers.iiiTABLEOFCONTENTSListofTables................................................................................................viListofFigures...........
4、.....................................................................................viiAbstract......................................................................................................ix1.IntroductionandBackground.......................................................
5、..................11.1Introduction...........................................................................................11.2DifferentMethodsforPackingRPLCColumns...................................21.2.1AxialCompression...........................................................
6、............31.2.2RadialCompression.....................................................................41.2.3SlurryPacking..............................................................................51.3DescriptorsofColumnPerformance...............................................
7、.....61.4HeterogeneityFoundWithinthePackedBedsofCurrentRPLCColumns...........................................................................................81.5ResearchGoals......................................................................................131.5.1CentripetalForc
8、easaToolforPackingRPLCColu