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1、上海大學(xué)碩士學(xué)位論文鋇鐵氧體磁光薄膜的制備與性能研究姓名:周炯申請(qǐng)學(xué)位級(jí)別:碩士專業(yè):光學(xué)指導(dǎo)教師:馬洪良20060501上海大學(xué)碩=E學(xué)位論文AbstractBariumferritehasattractedla塢ea札emionduetoitsexcellentchemistrystability,aJlti—causticity,hi曲aIlisotropya11dhi曲coercivityrecemyears.ThisfeHDmagneticmateriaIhasbeenwideIyappIiedinthemanufactllring
2、ofmagnetismandmagneto—opticdeVices.Firstly,血ebestmixtureratioofSol·gelmethodprecursorwaspreparedbychangingtheinitialfactorssuchlikedi丘毫rentFe/Bamolratio,molratioRofcitricacidtothenitrate,pHvaluea11dtl】eannealedtemperature.MagneticpowdersofBaFelI501825andBa(CoZr)xFell5—2xO28
3、25serieswerepr印ared.Then,cobaltnitrateandzirconiumnitratewereinnovativelyintroducedaccordingtothesubject.Magnetict11infilmsofBaFeH501825andBaFe2280442se“eswerepreparedbyusingSol—gelspinningandmagneto-opticthinfilmsofBa(CoZr)xFell5.2xol825serieswerepreparedbyPulsedLaserDepos
4、itjon(PLD)technique.Secondly,DSC/TGXRD,AFM,VSMandRamanSpectroscopicAnalysiswereutilizedtostudyonthebariumfbrritepowdeLthinfilmandthedopedsamples.Theresuhsshowedthecorrespondingsurfacemicrostmcture,magneticperformanceandR鋤anspectrum.Finally,putthe“nmmwimopticalrotationasmagn
5、et0—0pticmaterialdirectlybetweenpol捌zerandpolarizationa芏1alyzer,usingextinctionmethodtomeasuremagneto—opticeff毫ct,weobtainedthetransmissionratiocurve,mtationa1191eandmagneto—opticalflgureofmeritbychangingthewaVelengthoflaseLThemainexperimentalresultsasfollows:1、AsthebariLln
6、lferritcthiⅡ丘lm,t}lebestmagneticperforfnanceofBaFe2280442thinfilmwaspreparedundertheannealedtemperatureof1000℃whenpH=8aIldR=1.TheexperimentalresultexhibitedthattheperpendicularsquarenesswasO.60whilethein-plane’swas0.53.Theperpendjcularandin—plane’ssaturationmagnetizationsan
7、dcoercivitieswerel79em“cm3,47640ea11d198emu/cm5,36450e,respectiveIy.上海大學(xué)碩士學(xué)位論文2、AstheBa(Cozr)xFell5—2x01825magneticperfomlancewithdin、erem鋤ountofdoping,山ebestdoping鋤oum、vas0.2.Thein—plane’scoercivitywas10000e,whjleM§(1T)aildMrwas54cm毗mjaIld25em“cm3.耵leperpendiclll盯coercivit
8、ywas9500e,whileMs(1T)andM,was56emu/cm3and27em“cm3.3、Magneto·optice行bctwasmeasllred