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1、原始數(shù)據(jù)2015.03.18上午F3-200ulF412h一、氯化汞1、23#30#10:00—11:00取12ulF4---10mlNaCl,攪拌1min,立即取20ul、100ul測光值。同時(shí),取20ulF4立即測光值。文件名。加氯化汞(濃度:0.01-0.1mg/L),立即測光值,文件名<23-0.XLS><30-0.XLS>培養(yǎng)24h后測光值,文件名<23-1.XLS><30-1.XLS>。兩個(gè)板摞在一起,小號在上,大號用蓋子罩上2、3#7#10:00—11:00取12ulF4---10mlNaCl,攪拌1min,立
2、即取20ul、100ul測光值。同時(shí),取20ulF4立即測光值。文件名。加氯化汞(濃度:0.01-0.15mg/L),立即測光值,文件名<3-0.XLS><7-0.XLS>培養(yǎng)24h后測光值,文件名<3-1.XLS><7-1.XLS>。兩個(gè)板摞在一起,小號在上,大號用蓋子罩上二、硝酸鎘1、1#32#10:00—11:00取12ulF4---10mlNaCl,攪拌1min,立即取20ul、100ul測光值。同時(shí),取20ulF4立即測光值。文件名。加硝酸鎘(濃度:0.1-5mg/L),立即測光值,文件
3、名<1-0.XLS><32-0.XLS>培養(yǎng)24h后測光值,文件名<1-1.XLS><32-1.XLS>。兩個(gè)板摞在一起,小號在上,大號用蓋子罩上2、14#25#10:00—11:00取12ulF4---10mlNaCl,攪拌1min,立即取20ul、100ul測光值。同時(shí),取20ulF4立即測光值。文件名。加氯化汞(濃度:0.1-10mg/L),立即測光值,文件名<14-0.XLS><25-0.XLS>培養(yǎng)24h后測光值,文件名<14-1.XLS><25-1.XLS>。兩個(gè)板摞在一起,小號在上,大號用蓋子罩上結(jié)果初始光值來
4、源F410ulF4→10ml(1)10ulF4→20ml(2)10ulF4→10ml(1)10ulF4→20ml(2)時(shí)間1min1min1min40min40min體積20201002010020100201003.4E+3810.5837.0817.6160.832.4211.0210.5445.903.4E+3811.5236.4218.9561.702.9110.5310.7947.443.4E+3813.4541.3117.9460.362.9210.569.9948.28平均光值3.4E+381.094.750.602.820.261.22
5、0.130.74分析:平行性較好,但光值有點(diǎn)高,24h后的光值如下:一、氯化汞1、23#50.1921.9918.5939.455.5392.42286.960.02370.003348.6655.3032.9818.8987.5113.011.07984.130.01530.0046101.255.7134.1425.6060.1911.800.904068.600.02250.005998.6347.1324.7812.2980.832.1560.135886.270.10720.006879.9858.8825.8215.4657.872.948
6、0.1276104.20.00650.003958.5461.9624.9911.5148.799.9930.121254.140.00730.005346.37556281722、30#917.0695.0302.0590.845.540.4199932.40.06620.0443689.8941.0566.6315.6105181.040.6857499.20.05060.0565732.3690.0603.9281.8131.7412.80.446311110.08700.0680869.71025714.692.5012367.0150.214
7、3469.90.06330.0928963.7996.3400.8134.2879.69.3610.0718914.30.08490.0825806.0862.5550.097.39102513.210.193627.080.01460.098610239058196598473、3#52.0415.7517.3238.935.9610.561777.460.00310.00102.8343.83626.3431.1055.1615.086.10663.500.00490.002235.9322.2327.2013.8742.288.7290.4137
8、67.300.00750.003097.3134.4318.6811.1357.762.526